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PHASE ANALYSIS AND PHYSICAL PROPERTIES OF B2O3-ADDED ZIRCON CERAMICS SINTERED AT 1300 °C


 
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1. Title Title of document PHASE ANALYSIS AND PHYSICAL PROPERTIES OF B2O3-ADDED ZIRCON CERAMICS SINTERED AT 1300 °C
 
2. Creator Author's name, affiliation, country Fikriyatul Azizah Su'ud; Department of Physics, Science and Technology Faculty, Maulana Malik Ibrahim Malang Jl. Gajayana No. 50 Malang 65144, East Java; Indonesia
 
2. Creator Author's name, affiliation, country Suminar Pratapa; Department of Physics, Science and Analytical Data Faculty, Sepuluh Nopember Institute of Technology Jl. Teknik Kimia, Sukolilo Surabaya 60111, East Java; Indonesia
 
2. Creator Author's name, affiliation, country Musyarofah Musyarofah; Department of Physics, Science Faculty, Kalimantan Institute of Technology Jl. Soekarno Hatta No.KM 15 Kota Balikpapan 76127, East Kalimantan; Indonesia
 
3. Subject Discipline(s) Applied physics, Material, Nanomaterial
 
3. Subject Keyword(s) Ceramic; Zircon; Boria; Natural Sand
 
4. Description Abstract This study was aimed to know the effect of B2O3(boria) addition on the phase composition and physical properties of zircon ceramics.The raw zircon powder used in the study was a purified natural zircon sand from Kereng Pangi, Central Kalimantan, Indonesia. The zircon ceramics were prepared by a solid state reaction method with variation of B2O3 addition of 3 wt%, 6 wt% and 9 wt% and sintered at 1300 °C for 5h. The phase composition, density and microstructure were characterized using X-ray diffraction (XRD), densimeter and Scanning Electron Microscope (SEM), respectively. Vickers Hardness measurement was perfomed at the polished surface of the ceramics. Results showed that all samples contained pure zircon phase, i.e. there was no effect of B2O3 addition on the phase composition. In general, the density and hardness increased with increasing B2O3 addition, but addition up to 9 wt% is not optimum to achieve ultra-dense zircon ceramics. Furthermore, the SEM image also showed no significant difference in average grain size. The crystallite size has grown nearly eight times (325 nm) of its original powder. The Vickers hardness of the ceramics is not significantly influenced by the addition of boria. It appears that the boria failure to increase densification also results in the extent of contact between grains which then produces relatively large zircon grains.
 
5. Publisher Organizing agency, location Universitas Islam Negeri Maulana Malik Ibrahim Malang
 
6. Contributor Sponsor(s) Suminar Pratapa, ITS; Musyarofah, ITK
 
7. Date (YYYY-MM-DD) 2021-12-20
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://ejournal.uin-malang.ac.id/index.php/NEUTRINO/article/view/12663
 
10. Identifier Digital Object Identifier (DOI) https://doi.org/10.18860/neu.v14i1.12663
 
11. Source Title; vol., no. (year) Jurnal Neutrino:Jurnal Fisika dan Aplikasinya; Vol 14, No 1 (2021): October
 
12. Language English=en en
 
13. Relation Supp. Files
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c) 2021 Fikriyatul Azizah Su'ud, Suminar Pratapa, Musyarofah Musyarofah
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