SYNTHESIS AND CHARACTERIZATION OF CALCIUM SILICATE FROM RICE HUSK ASH AND SNAIL SHELL

Sadang Husain, Ninis Hadi Haryanti, Suryajaya Suryajaya, Antung Permitaria

Abstract


Calcium silicate ceramics have been made using natural ingredients such as rice husk and snail shell with solid reaction techniques. The aim of this study to determine the characteristics of calcium silicate that have been sintered at a temperature of 900 °C, 1000 °C, and 1100 °C. Samples were characterized by X-Ray Diffraction (XRD), optical microscopy, and Fourier Transform Infra-Red (FTIR). The results of XRD characterization showed that CaSiO3 (calcium silicate) along with the increase in calcination temperature and quantity was increased due to the increase of temperature of calcination. FTIR analysis showed that the Ca-Si-O bond was formed at wave number ranging from 848 cm-1 and 999 – 1001 cm-1.


Keywords


Calcium silicate; Rice husk ash; The shell of a snail

Full Text:

PDF

References


Sankar S, Sharma SK, Kim DY. Synthesis and characterization of mesoporous SiO 2 nanoparticles synthesized from Biogenic Rice Husk Ash for optoelectronic applications 1. An Int J Eng Sci. 2016;17(1):353–8.

Phuttawong R, Chantaramee N, Pookmanee P, Puntharod R. Synthesis and Characterization of Calcium Silicate from Rice Husk Ash and Shell of Snail Pomacea canaliculata by Solid State Reaction. Adv Mater Res. 2015;1103:1–7.

Felipe-Sesé M, Eliche-Quesada D, Corpas-Iglesias FA. The use of solid residues derived from different industrial activities to obtain calcium silicates for use as insulating construction materials. Ceram Int. 2011;37(8):3019–28.

Morales-Flórez V, Santos A, López A, Moriña I, Esquivias L. Calcium silicates synthesised from industrial residues with the ability for CO2 sequestration. Waste Manag Res. 2014;32(12):1178–85.

Leite FHG, Almeida TF, Faria RT, Holanda JNF. Synthesis and characterization of calcium silicate insulating material using avian eggshell waste. Ceram Int [Internet]. Elsevier; 2017;43(5):4674–9. Available from: http://dx.doi.org/10.1016/j.ceramint.2016.12.146

Ho CC, Wei CK, Lin SY, Ding SJ. Calcium silicate cements prepared by hydrothermal synthesis for bone repair. Ceram Int [Internet]. Elsevier; 2016;42(7):9183–9. Available from: http://dx.doi.org/10.1016/j.ceramint.2016.03.013

Yarusova SB, Mikhailov MM, Sushkov YV, Gordienko PS, Zhevtun IG, Banerjee S, et al. Effect of annealing conditions on the structure, phase and granulometry composition, and reflectance spectra and their changes on irradiation for calcium silicate powders. Mater Chem Phys. Elsevier B.V.; 2017;197:266–71.

Lee BS, Lin HP, Chan JCC, Wang WC, Hung PH, Tsai YH, et al. A novel sol-gel-derived calcium silicate cement with short setting time for application in endodontic repair of perforations. Int J Nanomedicine. 2018;13:261–71.

Meiszterics A, Rosta L, Peterlik H, Rohonczy J, Kubuki S, Henits P, et al. Structural characterization of gel-derived calcium silicate systems. J Phys Chem A. 2010;114(38):10403–11.

Meiszterics A, Sinkó K. Sol-gel derived calcium silicate ceramics. Colloids Surfaces A Physicochem Eng Asp. 2008;319(1–3):143–8.

Istiyati I, Asmi D. Fabrikasi dan Karakterisasi Keramik Kalsium Silikat Menggunakan Bahan Komersial Kalsium Oksida dan Silika dengan Reaksi Padatan pada Suhu 1300 ° C. J Teor dan Apl Fis. 2013;01(01):37–42.

Sholikha I, Friyatmoko WK, Dewi E, Utami S. Sintesis dan Karakterisasi Silika Gel dari Limbah Abu Sekam Padi ( Oryza Sativa ) dengan Variasi Konsentrasi Pengasaman. Pelita-Jurnal Penelit. 2010;1–13.

Budiman B, Asmi D. Sintesis Keramik Kalsium Silikat Menggunakan Kalsium Karbonat (CaCO3) dan Silikon Dioksida (SiO2) dengan Teknik Reaksi Padatan pada Suhu Sintering 1200 °C. J Teor dan Apl Fis. 2013;01(01):1–5.

Sari SNP, Asmi D. Fabrikasi dan Karakterisasi Keramik Kalsium Silikat Menggunakan Bahan Komersial Kalsium Oksida dan Silika dengan Reaksi Padatan pada Suhu 1000 °C. J Teor dan Apl Fis. 2013;01(01):53–7.

Ulfah, Asmi D. Gugus Fungsional , Mikrostruktur dan Struktur Keramik Kalsium Silikat Berbasis Silika Sekam Padi pada Suhu 1100 o C dengan Teknik Reaksi Padatan. J Teor dan Apl Fis. 2013;01(01):25–9.

Martinez A, Izquierdo-Barba I, Vallet-Regi M. Bioactivity of a CaO - SiO2 binary glasses system. Chem Mater. 2000;12(10):3080–8.

Bao Q, Zhao K, Liu J. Characterization of wollastonite coatings prepared by sol-gel on Ti substrate. J Coatings Technol Res. 2012;9(2):189–93.




DOI: https://doi.org/10.18860/neu.v11i2.6608

Refbacks

  • There are currently no refbacks.


Copyright (c) 2019 Sadang Husain, Ninis Hadi Haryanti, Suryajaya Suryajaya, Antung Permitaria

Creative Commons License
This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.

 

Published By:
Program Studi Fisika Fakultas Sains dan Teknologi Universitas Islam Negeri (UIN) Maulana Malik Ibrahim Malang, Indonesia
B.J. Habibie 2nd Floor
Jl. Gajayana No.50 Malang 65144
Telp./Fax.: (0341) 558933
Email: neutrino@uin-malang.ac.id

 

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License 

View My Stats